N-(tert-Butyldimethylsilyl)-N-methyl-trifluoroacetamide
Title | Journal |
---|---|
Determination of hydroxylated metabolites of polycyclic aromatic hydrocarbons in sediment samples by combining subcritical water extraction and dispersive liquid-liquid microextraction with derivatization. | Analytica chimica acta 20121113 |
Determination of Δ9-tetrahydrocannabinol and 11-nor-9-carboxy-Δ9-tetrahydrocannabinol in water samples by solid-phase microextraction with on-fiber derivatization and gas chromatography-mass spectrometry. | Journal of chromatography. A 20120706 |
Gas chromatography-mass spectrometry method for the determination of free amino acids as their dimethyl-tert-butylsilyl (TBDMS) derivatives in animal source food. | Journal of agricultural and food chemistry 20120314 |
Resolving phenylalanine metabolism sheds light on natural synthesis of penicillin G in Penicillium chrysogenum. | Eukaryotic cell 20120201 |
Analysis of endocrine disrupting compounds, pharmaceuticals and personal care products in sewage sludge by gas chromatography-mass spectrometry. | Talanta 20120130 |
Measurement of hepatic protein fractional synthetic rate with stable isotope labeling technique in thapsigargin stressed HepG2 cells. | International journal of biological sciences 20120101 |
Metabolic pathway confirmation and discovery through (13)C-labeling of proteinogenic amino acids. | Journal of visualized experiments : JoVE 20120101 |
Selection of the derivatization reagent--the case of human blood cholesterol, its precursors and phytosterols GC-MS analyses. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20111215 |
Simultaneous analysis of pesticides from different chemical classes by using a derivatisation step and gas chromatography-mass spectrometry. | Journal of chromatography. A 20111104 |
Excretion of 2,3-dihydroxy-propionamide (OH-PA), the hydrolysis product of glycidamide, in human urine after single oral dose of deuterium-labeled acrylamide. | Archives of toxicology 20110601 |
Simultaneous determination of 2-naphthol and 1-hydroxy pyrene in urine by gas chromatography-mass spectrometry. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20110301 |
Analytical method for assessing potential dermal exposure to pesticides of a non-agricultural occupationally exposed population. | Analytical and bioanalytical chemistry 20110101 |
A fully validated method for the determination of vardenafil in blood using gas chromatography/mass spectrometry. | Journal of mass spectrometry : JMS 20110101 |
Stable isotopic profiling of intermediary metabolic flux in developing and adult stage Caenorhabditis elegans. | Journal of visualized experiments : JoVE 20110101 |
Rapeseed and milk protein exhibit a similar overall nutritional value but marked difference in postprandial regional nitrogen utilization in rats. | Nutrition & metabolism 20110101 |
Catabolic regulation analysis of Escherichia coli and its crp, mlc, mgsA, pgi and ptsG mutants. | Microbial cell factories 20110101 |
Metabolic engineering of the L-phenylalanine pathway in Escherichia coli for the production of S- or R-mandelic acid. | Microbial cell factories 20110101 |
An empirical Bayes model using a competition score for metabolite identification in gas chromatography mass spectrometry. | BMC bioinformatics 20110101 |
Determination of synthetic phenolic antioxidants and their metabolites in water samples by downscaled solid-phase extraction, silylation and gas chromatography-mass spectrometry. | Journal of chromatography. A 20101008 |
Useful second-tier tests in expanded newborn screening of isovaleric acidemia and methylmalonic aciduria. | Journal of inherited metabolic disease 20101001 |
Determination of triclosan and methyl triclosan in environmental solid samples by matrix solid-phase dispersion and gas chromatography-mass spectrometry. | Journal of separation science 20100901 |
Artifacts related to N-methyl-N-(tert-butyldimethylsilyl)trifluoroacetamide derivatization of citrulline revealed by gas chromatography-mass spectrometry using both electron and chemical ionization. | Journal of chromatography. A 20100813 |
Trimethylsilyldiazomethane (TMSD) as a new derivatization reagent for trace analysis of selected non-steroidal anti-inflammatory drugs (NSAIDs) by gas chromatography methods. | Analytical and bioanalytical chemistry 20100801 |
In-sample acetylation-non-porous membrane-assisted liquid-liquid extraction for the determination of parabens and triclosan in water samples. | Analytical and bioanalytical chemistry 20100701 |
Determination of butoxyacetic acid (biomarker of ethylene glycol monobutyl ether exposure) in human urine candidate reference material. | Analytical and bioanalytical chemistry 20100501 |
11-nor-Delta9-tetrahydrocannabinol-9-carboxylic acid ethyl ester (THC-COOEt): unsuccessful search for a marker of combined cannabis and alcohol consumption. | Forensic science international 20100320 |
Optimization of N-methyl-N-[tert-butyldimethylsilyl]trifluoroacetamide as a derivatization agent for determining isotopic enrichment of glycerol in very-low density lipoproteins. | Rapid communications in mass spectrometry : RCM 20100315 |
Trace analysis of free and combined amino acids in atmospheric aerosols by gas chromatography-mass spectrometry. | Journal of chromatography. A 20100101 |
Quantitation of benzodiazepines in blood and urine using gas chromatography-mass spectrometry (GC-MS). | Methods in molecular biology (Clifton, N.J.) 20100101 |
Multivariate modeling identifies neutrophil- and Th17-related factors as differential serum biomarkers of chronic murine colitis. | PloS one 20100101 |
Development and validation of a gas chromatography/mass spectrometry method for the assessment of genomic DNA methylation. | Rapid communications in mass spectrometry : RCM 20090901 |
One-step extraction and derivatization liquid-phase microextraction for the determination of chlorophenols by gas chromatography-mass spectrometry. | Journal of chromatography. A 20090828 |
Evaluation of principal cannabinoids in airborne particulates. | Analytica chimica acta 20090508 |
Comparison of MTBSTFA and BSTFA in derivatization reactions of polar compounds prior to GC/MS analysis. | Talanta 20090215 |
The detection of various opiates and benzodiazepines by comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry. | Rapid communications in mass spectrometry : RCM 20090201 |
Dispersive liquid-liquid microextraction applied to the simultaneous derivatization and concentration of triclosan and methyltriclosan in water samples. | Journal of chromatography. A 20090109 |
Determination of creatine and guanidinoacetate by GC-MS: study of their stability in urine at different temperatures. | Clinical biochemistry 20090101 |
Uric acid is a mediator of the Plasmodium falciparum-induced inflammatory response. | PloS one 20090101 |
The effect of high glucocorticoid administration and food restriction on rodent skeletal muscle mitochondrial function and protein metabolism. | PloS one 20090101 |
[Determination of chlorpyrifos and its metabolite in vegetables using gas chromatography-tandem mass spectrometry]. | Se pu = Chinese journal of chromatography 20090101 |
Susceptibility of pancreatic beta cells to fatty acids is regulated by LXR/PPARalpha-dependent stearoyl-coenzyme A desaturase. | PloS one 20090101 |
Solid phase microextraction procedure for the determination of alkylphenols in water by on-fiber derivatization with N-tert-butyl-dimethylsilyl-N-methyltrifluoroacetamide. | Analytica chimica acta 20080829 |
Simultaneous determination of pharmaceuticals, endocrine disrupting compounds and hormone in soils by gas chromatography-mass spectrometry. | Journal of chromatography. A 20080822 |
Identification and quantification of ibuprofen, naproxen, ketoprofen and diclofenac present in waste-waters, as their trimethylsilyl derivatives, by gas chromatography mass spectrometry. | Talanta 20080730 |
Simplified sample preparation method for triclosan and methyltriclosan determination in biota and foodstuff samples. | Journal of chromatography. A 20080425 |
Differential metabolomics using stable isotope labeling and two-dimensional gas chromatography with time-of-flight mass spectrometry. | Analytical chemistry 20080101 |
Simultaneous analysis of lysine, Nepsilon-carboxymethyllysine and lysinoalanine from proteins. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20071201 |
Optimisation of the on-fibre derivatisation of volatile fatty acids in the simultaneous determination together with phenols and indoles in cow slurries. | Analytical and bioanalytical chemistry 20071101 |
Derivatization of organophosphorus nerve agent degradation products for gas chromatography with ICPMS and TOF-MS detection. | Analytical and bioanalytical chemistry 20070601 |
Changes in the sugarcane metabolome with stem development. Are they related to sucrose accumulation? | Plant & cell physiology 20070401 |
Determination of parabens and triclosan in indoor dust using matrix solid-phase dispersion and gas chromatography with tandem mass spectrometry. | Analytical chemistry 20070215 |
Fluxome analysis using GC-MS. | Microbial cell factories 20070101 |
Highly selective sample preparation and gas chromatographic-mass spectrometric analysis of chlorpyrifos, diazinon and their major metabolites in sludge and sludge-fertilized agricultural soils. | Journal of chromatography. A 20061103 |
Determination of nitrogen mustard hydrolysis products, ethanolamines by gas chromatography-mass spectrometry after tert-butyldimethylsilyl derivatization. | Journal of chromatography. A 20060728 |
Fast gas chromatography-negative-ion chemical ionization mass spectrometry with microscale volume sample preparation for the determination of benzodiazepines and alpha-hydroxy metabolites, zaleplon and zopiclone in whole blood. | Journal of mass spectrometry : JMS 20060601 |
Determination of ethephon residues in water by gas chromatography with cubic mass spectrometry after ion-exchange purification and derivatisation with N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide. | Journal of chromatography. A 20060303 |
Optimization of silylation using N-methyl-N-(trimethylsilyl)-trifluoroacetamide, N,O-bis-(trimethylsilyl)-trifluoroacetamide and N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide for the determination of the estrogens estrone and 17alpha-ethinylestradiol by gas chromatography-mass spectrometry. | Journal of chromatography. A 20060303 |
Analysis of tert-butyldimethylsilyl derivatives in heavy gas oil from Brazilian naphthenic acids by gas chromatography coupled to mass spectrometry with electron impact ionization. | Journal of chromatography. A 20060210 |
Neurochemical analysis of amino acids, polyamines and carboxylic acids: GC-MS quantitation of tBDMS derivatives using ammonia positive chemical ionization. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20060202 |
A validated positive chemical ionization GC/MS method for the identification and quantification of amphetamine, opiates, cocaine, and metabolites in human postmortem brain. | Journal of mass spectrometry : JMS 20060201 |
Comparison and evaluation of analysis procedures for the quantification of (2-methoxyethoxy)acetic acid in urine. | Analytical and bioanalytical chemistry 20050901 |
Simultaneous retention index analysis of urinary amino acids and carboxylic acids for graphic recognition of abnormal state. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20050705 |
Validated toxicological determination of 30 drugs of abuse as optimized derivatives in oral fluid by long column fast gas chromatography/electron impact mass spectrometry. | Journal of mass spectrometry : JMS 20050601 |
Determination of 14 benzodiazepines and hydroxy metabolites, zaleplon and zolpidem as tert-butyldimethylsilyl derivatives compared with other common silylating reagents in whole blood by gas chromatography-mass spectrometry. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20050425 |
Optimization of solid-phase microextraction conditions for the determination of triclosan and possible related compounds in water samples. | Journal of chromatography. A 20050422 |
Application of gas chromatography-mass spectrometry for the determination of urinary ethylenethiourea in humans. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20050125 |
Determination and quantification of alpha,beta,gamma,delta-unsaturated aldehydes as pentafluorobenzyl-oxime derivates in diatom cultures and natural phytoplankton populations: application in marine field studies. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20050105 |
Determination of thiodiglycol, a mustard gas hydrolysis product by gas chromatography-mass spectrometry after tert-butyldimethylsilylation. | Journal of chromatography. A 20041224 |
A multiresidue method for the analysis of phenols and nitrophenols in the atmosphere. | Journal of environmental monitoring : JEM 20041201 |
Analysis of heterocyclic aromatic amines in foods by gas chromatography-mass spectrometry as their tert.-butyldimethylsilyl derivatives. | Journal of chromatography. A 20040618 |
Determination of picogram levels of midazolam, and 1- and 4-hydroxymidazolam in human plasma by gas chromatography-negative chemical ionization-mass spectrometry. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20040405 |
Development of a gas chromatographic test for the quantification of the biomarker 3-bromopropionic acid in human urine. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20040405 |
Suitability of N,O-bis(trimethylsilyl)trifluoroacetamide and N-(tert-butyldimethylsilyl)-N-methyltrifluoroacetamide as derivatization reagents for the determination of the estrogens estrone and 17alpha-ethinylestradiol by gas chromatography-mass spectrometry. | Journal of chromatography. A 20040213 |
Solid-phase microextraction with on-fiber derivatization for the analysis of anti-inflammatory drugs in water samples. | Journal of chromatography. A 20040123 |
Quantification of bacterial lipopolysaccharides (endotoxin) by GC-MS determination of 3-hydroxy fatty acids. | Journal of environmental monitoring : JEM 20040101 |
Analysis of O,S-dimethyl hydrogen phosphorothioate in urine, a specific biomarker for methamidophos. | Journal of agricultural and food chemistry 20031008 |
13C enrichment of extracellular neurotransmitter glutamate in rat brain--combined mass spectrometry and NMR studies of neurotransmitter turnover and uptake into glia in vivo. | Cellular and molecular biology (Noisy-le-Grand, France) 20030701 |
Determination of the herbicide glyphosate and its metabolite in biological specimens by gas chromatography-mass spectrometry. A case of poisoning by roundup herbicide. | Journal of analytical toxicology 20030401 |
Application of spectroscopic and computational methods in the study of the electronic excitations of partially silylated hydroxyquinones. | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy 20030315 |
Simultaneous determination of methionine sulfoxide and methionine in blood plasma using gas chromatography-mass spectrometry. | Analytical biochemistry 20030201 |
Determination of acidic drugs in sewage water by gas chromatography-mass spectrometry as tert.-butyldimethylsilyl derivatives. | Journal of chromatography. A 20030124 |
Stable isotope dilution method for the determination of guanidinoacetic acid by gas chromatography/mass spectrometry. | Rapid communications in mass spectrometry : RCM 20030101 |
Gas chromatography-mass spectrometry method for determination of phenylalanine and tyrosine in neonatal blood spots. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20021125 |
In vivo microdialysis and gas-chromatography/mass-spectrometry for 13C-enrichment measurement of extracellular glutamate in rat brain. | Journal of neuroscience methods 20021030 |
New gas chromatographic-mass spectrometric method for the determination of urinary pyrethroid metabolites in environmental medicine. | Journal of chromatography. B, Analytical technologies in the biomedical and life sciences 20021005 |
Analysis of glycated and ascorbylated proteins by gas chromatography-mass spectrometry. | Journal of agricultural and food chemistry 20020925 |
Assay of serum allantoin in humans by gas chromatography-mass spectrometry. | Clinica chimica acta; international journal of clinical chemistry 20020401 |
Separation, identification, and quantification of amino acids in L-lysine fermentation potato juices by gas chromatography-mass spectrometry. | Fresenius' journal of analytical chemistry 20011001 |
Analysis of 3,5,6-trichloro-2-pyridinol in urine samples from the general population using gas chromatography-mass spectrometry after steam distillation and solid-phase extraction. | Journal of chromatography. B, Biomedical sciences and applications 20010805 |
Determination of thiodyglycol in groundwater using solid-phase extraction followed by gas chromatography with mass spectrometric detection in the selected-ion mode. | Journal of chromatography. A 20010309 |